Technology Process of C18H17NO5
There total 3 articles about C18H17NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
formic acid; C17H17NO4;
With
sodium formate; acetic anhydride;
at 20 ℃;
for 4h;
With
hydrogenchloride;
In
methanol; water;
at 20 ℃;
for 24h;
DOI:10.1016/j.ejmech.2010.11.025
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium acetate; acetic acid / 20 h / 20 °C
2: sodium formate; acetic anhydride / 4 h / 20 °C
With
sodium formate; sodium acetate; acetic anhydride; acetic acid;
1: |Pictet-Spengler Synthesis;
DOI:10.1016/j.cclet.2013.02.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride / 72 h / 20 °C
2: sodium acetate; acetic acid / 20 h / 20 °C
3: sodium formate; acetic anhydride / 4 h / 20 °C
With
thionyl chloride; sodium formate; sodium acetate; acetic anhydride; acetic acid;
2: |Pictet-Spengler Synthesis;
DOI:10.1016/j.cclet.2013.02.014