methyl 2,3-diacetoxy-5-chlorophenylacetate

Base Information

Chemical Name:methyl 2,3-diacetoxy-5-chlorophenylacetate
CAS No.:86232-50-0
Molecular Formula:C₁₃H₁₃ClO₆
Molecular Weight:300.696
Hs Code.:

Synonyms:

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Chemical Property of methyl 2,3-diacetoxy-5-chlorophenylacetate

Chemical Property:

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Technology Process of methyl 2,3-diacetoxy-5-chlorophenylacetate

There total 16 articles about methyl 2,3-diacetoxy-5-chlorophenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 86232-49-7
methyl 5-chloro-2,3-dihydroxyphenylacetate

: 75-36-5
acetyl chloride

: 86232-50-0
methyl 2,3-diacetoxy-5-chlorophenylacetate

Guidance literature:: Heating;

Reference yield:

: 7740-05-8
5-chloro-2-hydroxy-3-methoxy-benzaldehyde

: 86232-50-0
methyl 2,3-diacetoxy-5-chlorophenylacetate

Guidance literature:: Multi-step reaction with 9 steps

1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h

2: 75 percent / K₂CO₃ / acetone / 5 h / Heating

3: 77 percent / KMnO₄ / H₂O / 5 h / Heating

4: SOCl₂ / 2 h / Heating

5: diethyl ether / 10 h / 20 °C

6: 45 percent / silver oxide / dioxane; H₂O / 1 h / 95 °C

7: 88 percent / AlBr₃ / benzene / 3 h / Heating

8: 91 percent / conc. H₂SO₄ / 1,2-dichloro-ethane

9: 85 percent / Heating

With potassium hydroxide; potassium permanganate; thionyl chloride; aluminum tri-bromide; sulfuric acid; potassium carbonate; hydrazine hydrate; silver(l) oxide; In 1,4-dioxane; diethyl ether; water; 1,2-dichloro-ethane; acetone; benzene;

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 86232-50-0
methyl 2,3-diacetoxy-5-chlorophenylacetate

Guidance literature:: Multi-step reaction with 10 steps

1: 45 percent / chlorine / acetic acid / 5 h / 20 °C

2: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h

3: 75 percent / K₂CO₃ / acetone / 5 h / Heating

4: 77 percent / KMnO₄ / H₂O / 5 h / Heating

5: SOCl₂ / 2 h / Heating

6: diethyl ether / 10 h / 20 °C

7: 45 percent / silver oxide / dioxane; H₂O / 1 h / 95 °C

8: 88 percent / AlBr₃ / benzene / 3 h / Heating

9: 91 percent / conc. H₂SO₄ / 1,2-dichloro-ethane

10: 85 percent / Heating

With potassium hydroxide; potassium permanganate; thionyl chloride; aluminum tri-bromide; sulfuric acid; chlorine; potassium carbonate; hydrazine hydrate; silver(l) oxide; In 1,4-dioxane; diethyl ether; water; acetic acid; 1,2-dichloro-ethane; acetone; benzene;