triphenylantimony dithiocyanate

Base Information

Chemical Name:triphenylantimony dithiocyanate
CAS No.:24692-08-8
Molecular Formula:C₂₀H₁₅N₂S₂Sb
Molecular Weight:469.234
Hs Code.:

Synonyms:

Suppliers and Price of triphenylantimony dithiocyanate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylantimony dithiocyanate

Chemical Property:

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Technology Process of triphenylantimony dithiocyanate

There total 4 articles about triphenylantimony dithiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16681-13-3
chlorine isothiocyanate

: 603-36-1
triphenylantimony

: 24692-08-8,34716-93-3
triphenylantimony diisothiocyanate

: 594-31-0,34716-91-1,20265-29-6
triphenylantimony dichloride

Guidance literature:: In dichloromethane; stirring equimolar amts. (0°C, 10 min); fractional crystn.;
DOI:10.1016/0022-328X(95)05775-K

Reference yield:

: 603-36-1
triphenylantimony

: 592-87-0
lead(II) thiocyanate

: 24692-08-8,34716-93-3
triphenylantimony dithiocyanate

Guidance literature:: With Br₂; In dichloromethane; treatment of Pb(SCN)2 with Br2, cooling to 0°C, addn. to equimolar amt. of Sb-compd., stirring (0°C, 30 min); concn. (vac.), crystn. (freezer), collection, recrystn. (CHCl3/hexane=1:1), collection, washing (ether) or drying at 50°C in vac. (not specified); elem. anal.;
DOI:10.1016/0022-328X(95)05775-K