Technology Process of C22H35N3O7Si
There total 6 articles about C22H35N3O7Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium chloride; sodium azide / methanol; water / 72 h / 80 °C
2: pyridine / dichloromethane
With
pyridine; sodium azide; ammonium chloride;
In
methanol; dichloromethane; water;
DOI:10.1016/j.tet.2013.07.018
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium hydrogencarbonate; dihydrogen peroxide / acetonitrile / 4 h / 20 °C
2: 1H-imidazole / dichloromethane / 4 h / 0 °C
3: silver(l) oxide / N,N-dimethyl-formamide / 23 h / 20 °C / Inert atmosphere
4: ammonium chloride; sodium azide / methanol; water / 72 h / 80 °C
5: pyridine / dichloromethane
With
pyridine; 1H-imidazole; sodium azide; dihydrogen peroxide; ammonium chloride; potassium hydrogencarbonate; silver(l) oxide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2013.07.018
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydrogencarbonate; urea hydrogen peroxide adduct / acetonitrile / 70.5 h / 40 °C
2: silver(l) oxide / N,N-dimethyl-formamide / 23 h / 20 °C / Inert atmosphere
3: ammonium chloride; sodium azide / methanol; water / 72 h / 80 °C
4: pyridine / dichloromethane
With
pyridine; sodium azide; urea hydrogen peroxide adduct; ammonium chloride; potassium hydrogencarbonate; silver(l) oxide;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2013.07.018