1,4-butanediol, tBDMS

Base Information

Chemical Name:1,4-butanediol, tBDMS
CAS No.:122795-01-1
Molecular Formula:C16H38O2Si2
Molecular Weight:318.648
Hs Code.:
DSSTox Substance ID:DTXSID90423966
Wikidata:Q82236338
Mol file:122795-01-1.mol

Synonyms:1,4-butanediol, tBDMS;122795-01-1;1,4-Butanediol, bis-DMTBS;SCHEMBL8063404;DTXSID90423966;FQBZLVHZDYXUDM-UHFFFAOYSA-N;D87352;2,2,3,3,10,10,11,11-OCTAMETHYL-4,9-DIOXA-3,10-DISILADODECANE

Suppliers and Price of 1,4-butanediol, tBDMS

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,4-butanediol, tBDMS

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:9
Exact Mass:318.24103352
Heavy Atom Count:20
Complexity:256

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C)(C)OCCCCO[Si](C)(C)C(C)(C)C

Technology Process of 1,4-butanediol, tBDMS

There total 1 articles about 1,4-butanediol, tBDMS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 106-41-2
4-bromo-phenol

: 86864-60-0
2-(tert-butyldimethylsilyloxy)ethyl bromide

: 92-88-6
4,4'-Dihydroxybiphenyl

: 17348-65-1
di(methyl)tert-butyl(ethoxy)silane

: 122795-01-1
1,4-Bis-(tert-butyl-dimethyl-silanyloxy)-butane

: 96013-76-2
4-[2-(tert-butyldimethylsilyloxy)ethyl]phenol

: 108-95-2,27073-41-2
phenol

Guidance literature:: With pyridine; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; 4,4'-Dimethoxy-2,2'-bipyridin; NiI₂*3.5H₂O; sodium iodide; zinc; at 20 - 60 ℃; for 16h; chemoselective reaction;
DOI:10.1021/ja301769r

Reference yield: 98.0%

: 122795-01-1
1,4-Bis-(tert-butyl-dimethyl-silanyloxy)-butane

: 110-63-4
Butane-1,4-diol

Guidance literature:: sulfated SnO₂; In methanol; at 20 ℃; for 0.166667h;
DOI:10.1080/00397910701767056

Reference yield: 50.0%

: 122795-01-1
1,4-Bis-(tert-butyl-dimethyl-silanyloxy)-butane

: 100-52-7
benzaldehyde

: 19224-27-2
1,4-bis(benzoyloxy)butane

Guidance literature:: With Bromotrichloromethane; In acetonitrile; at 20 ℃; for 28h; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.8b02537