1,2-dimethoxy-3-(2-phenylvinyl)benzene

Base Information

Chemical Name:1,2-dimethoxy-3-(2-phenylvinyl)benzene
CAS No.:122950-70-3
Molecular Formula:C16H16O2
Molecular Weight:240.302
Hs Code.:
Mol file:122950-70-3.mol

Synonyms:(E)-3-fluorostilbene;(E)-2,3-Dimethoxystilbene;1,2-Dimethoxy-3-((E)-styryl)-benzene;

Suppliers and Price of 1,2-dimethoxy-3-(2-phenylvinyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-dimethoxy-3-(2-phenylvinyl)benzene

Chemical Property:

PSA：18.46000
LogP:3.87420

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 1,2-dimethoxy-3-(2-phenylvinyl)benzene

There total 5 articles about 1,2-dimethoxy-3-(2-phenylvinyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 100-39-0
benzyl bromide

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 122950-70-3
trans-2,3-dimethoxystilbene

Guidance literature:: benzyl bromide; With triethyl phosphite; at 130 ℃; for 5h;

With sodium methylate; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

2,3-dimethyoxybenzaldehyde; In N,N-dimethyl-formamide; at 20 - 100 ℃;
DOI:10.3390/molecules19079577

Reference yield:

: 1080-32-6
O,O-diethyl benzylphosphonate

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 122950-70-3
trans-2,3-dimethoxystilbene

Guidance literature:: O,O-diethyl benzylphosphonate; With 18-crown-6 ether; sodium methylate; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

2,3-dimethyoxybenzaldehyde; In N,N-dimethyl-formamide; at 20 - 120 ℃; for 6h;
DOI:10.1021/jm060630x

Reference yield:

: 1100-88-5
benzyltriphenylphosphonium chloride

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 122950-70-3
trans-2,3-dimethoxystilbene

Guidance literature:: With iodine; sodium methylate; Yield given. Multistep reaction; 1.) methanol, RT, 2.) toluene, irradiation;
DOI:10.1021/jo00280a032