Technology Process of Borate(1-), tetrakis(3-Methylphenyl)-, sodiuM(1:1)
There total 3 articles about Borate(1-), tetrakis(3-Methylphenyl)-, sodiuM(1:1) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
meta-bromotoluene;
With
iodine; magnesium;
In
diethyl ether;
at 20 ℃;
for 2.5h;
sodium tetrafluoroborate;
In
diethyl ether;
at 20 ℃;
for 42h;
DOI:10.1021/ja905432x
- Guidance literature:
-
sodium tetrafluoroborate;
With
magnesium;
In
tetrahydrofuran; ethylene dibromide;
for 0.0166667h;
Sealed tube;
Inert atmosphere;
Schlenk technique;
3-methylphenyl halide;
In
tetrahydrofuran; ethylene dibromide;
at 20 ℃;
for 12h;
Sealed tube;
Inert atmosphere;
Schlenk technique;
DOI:10.1002/anie.201501992
- Guidance literature:
-
In
xylene;
at temp. below 30°C under N2;