4-benzyloxy-2-dimethylaminopyrimidine

Base Information

Chemical Name:4-benzyloxy-2-dimethylaminopyrimidine
CAS No.:19810-62-9
Molecular Formula:C₁₃H₁₅N₃O
Molecular Weight:229.282
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-benzyloxy-2-dimethylaminopyrimidine

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Technology Process of 4-benzyloxy-2-dimethylaminopyrimidine

There total 3 articles about 4-benzyloxy-2-dimethylaminopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 108381-28-8
4-(benzyloxy)-2-chloropyrimidine

: 124-40-3
dimethyl amine

: 19810-62-9
4-benzyloxy-2-dimethylaminopyrimidine

Guidance literature:: In water; acetonitrile; at 100 ℃; for 1.5h; Autoclave;
DOI:10.1002/chem.201702877

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 19810-62-9
4-benzyloxy-2-dimethylaminopyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / Reflux

1.2: 13 h / -50 - 20 °C

2.1: water; acetonitrile / 1.5 h / 100 °C / Autoclave

With potassium tert-butylate; In tetrahydrofuran; water; acetonitrile;
DOI:10.1002/chem.201702877