1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)-

Base Information

Chemical Name:1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)-
CAS No.:124717-60-8
Molecular Formula:C10H11BrO2
Molecular Weight:243.1
Hs Code.:
DSSTox Substance ID:DTXSID10459863
Wikidata:Q82283735
Mol file:124717-60-8.mol

Synonyms:124717-60-8;2-(3-bromo-4-methylphenyl)-1,3-dioxolane;1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)-;SCHEMBL2856571;DTXSID10459863;YTQXPAWDHPRBBM-UHFFFAOYSA-N;MFCD27942538;2-(3-Bromo-4-methylphenyl)[1,3]dioxolane;CS-0193362;FT-0754131;E93217

Suppliers and Price of 1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:241.99424
Heavy Atom Count:13
Complexity:168

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)C2OCCO2)Br

Technology Process of 1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)-

There total 2 articles about 1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 36276-24-1
3-bromo-4-methyl-benzaldehyde

: 107-21-1
ethylene glycol

: 124717-60-8
3-bromo-4-methylbenzaldehyde ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 2h; Heating;
DOI:10.1021/jm00165a014

Reference yield:

: 36276-24-1
3-bromo-4-methyl-benzaldehyde

: 104-15-4
toluene-4-sulfonic acid

: 124717-60-8
3-bromo-4-methylbenzaldehyde ethylene acetal

Guidance literature:: In ethylene glycol; toluene;

Reference yield:

: 624-92-0
Dimethyldisulphide

: 124717-60-8
3-bromo-4-methylbenzaldehyde ethylene acetal

: 315188-39-7
2-[4-methyl-3-(methylsulfanyl)phenyl]-1,3-dioxolane

Guidance literature:: 3-bromo-4-methylbenzaldehyde ethylene acetal; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

Dimethyldisulphide; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1021/jm030356w