ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

Base Information

Chemical Name:ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate
CAS No.:74875-23-3
Molecular Formula:C₁₆H₁₇Cl₂N₅O₆S
Molecular Weight:478.313
Hs Code.:

ethyl N-<<<cyano<3,5-dichloro-4-(morpholinylsulfonyl)phenyl>hydrazinylidene>methyl>carbonyl>carbamate

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Chemical Property of ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

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Technology Process of ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

There total 3 articles about ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74875-17-5
2,6-dichloro-4-nitrobenzenesulfonyl chloride

: 74875-23-3
ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.64 g / diethyl ether / 3 h / Heating

2: 73 percent / SnCl₂*2H₂O, conc. aq. HCl / 1.25 h / Heating

3: 1.) 6 N aq. HCl, NaNO₂, 2.) pyridine / 1.) from 0 to 5 deg C, 2.) RT, 16 h

With pyridine; hydrogenchloride; tin(ll) chloride; sodium nitrite; In diethyl ether;
DOI:10.1021/jm00184a005

Reference yield:

: 74875-18-6
3,5-dichloro-4-(morpholinylsulfonyl)nitrobenzene

: 74875-23-3
ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / SnCl₂*2H₂O, conc. aq. HCl / 1.25 h / Heating

2: 1.) 6 N aq. HCl, NaNO₂, 2.) pyridine / 1.) from 0 to 5 deg C, 2.) RT, 16 h

With pyridine; hydrogenchloride; tin(ll) chloride; sodium nitrite;
DOI:10.1021/jm00184a005

Reference yield:

: 6629-04-5
ethyl N-cyanoacetylcarbamate

: 74875-19-7
3,5-dichloro-4-(morpholinylsulfonyl)aniline

: 74875-23-3
ethyl N-<<hydrazinylidene>methyl>carbonyl>carbamate

Guidance literature:: With pyridine; hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 1.) from 0 to 5 deg C, 2.) RT, 16 h;
DOI:10.1021/jm00184a005