BClN(C₆H₃(CH(CH₃)2)2)CH₂CH₂CH₂CH₂O

Base Information

• Chemical Name: BClN(C₆H₃(CH(CH₃)2)2)CH₂CH₂CH₂CH₂O
• CAS No.: 1072955-34-0
• Molecular Formula: C₁₆H₂₅BClNO
• Molecular Weight: 293.645
• Mol file: 1072955-34-0.mol

Synonyms:

Chemical Property of BClN(C₆H₃(CH(CH₃)2)2)CH₂CH₂CH₂CH₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BClN(C₆H₃(CH(CH₃)2)2)CH₂CH₂CH₂CH₂O

There total 3 articles about BClN(C₆H₃(CH(CH₃)2)2)CH₂CH₂CH₂CH₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + lithium (2,6-diisopropylphenyl)amide → BClN(C6H3(CH(CH3)2)2)CH2CH2CH2CH2O (1072955-34-0) + 2,6-diisopropylaniline hydrochloric acid salt (50522-40-2)

Guidance literature:

With boron trichloride; In hexane; at 20 ℃; for 18h;

DOI:10.1039/b810319d

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + 2,6-diisopropylbenzenamine (24544-04-5) → Cl2B(NHDipp) + BClN(C6H3(CH(CH3)2)2)CH2CH2CH2CH2O (1072955-34-0) + ClB(NHBipp)2 (1071097-44-3)

Guidance literature:

With boron trichloride; In tetrahydrofuran; for 18h;

DOI:10.1039/b810319d

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + boron trichloride (10294-34-5) + lithium (2,6-diisopropylphenyl)amide → BClN(C6H3(CH(CH3)2)2)CH2CH2CH2CH2O (1072955-34-0)

Guidance literature:

In tetrahydrofuran; soln. LiN(H)Dipp in THF was added to soln. BCl3 in n-hexane (1:1) at -80°C, allowed to warm to room temp. and stirred for 18 h; volatiles were removed in vacuo, residue was extd. with n-hexane;

DOI:10.1039/b810319d

upstream raw materials:

tetrahydrofuran

boron trichloride

2,6-diisopropylbenzenamine