3,4-Bis(trimethylsilyl)furan

Base Information

• Chemical Name: 3,4-Bis(trimethylsilyl)furan
• CAS No.: 126386-46-7
• Molecular Formula: C10H20OSi2
• Molecular Weight: 212.439
• DSSTox Substance ID: DTXSID80454289
• Nikkaji Number: J592.724B
• Wikidata: Q82275726
• Mol file: 126386-46-7.mol

Synonyms:3,4-Bis(trimethylsilyl)furan;Silane, 3,4-furandiylbis[trimethyl-;126386-46-7;3,4-di(trimethylsilyl)furan;SCHEMBL4572707;DTXSID80454289;KQKGLWMJTTXASS-UHFFFAOYSA-N

Chemical Property of 3,4-Bis(trimethylsilyl)furan

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 212.10526833
• Heavy Atom Count: 13
• Complexity: 158

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C)(C)C1=COC=C1[Si](C)(C)C

Technology Process of 3,4-Bis(trimethylsilyl)furan

There total 1 articles about 3,4-Bis(trimethylsilyl)furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-phenyl-1,3-oxazole (20662-89-9) + Bis(trimethylsilyl)ethyne (14630-40-1) → benzonitrile (100-47-0) + 3,4-Bis(trimethylsilyl)furan (126386-46-7)

Guidance literature:

at 300 ℃;

DOI:10.1039/c39890001238

Reference yield: 73.0%

3,4-Bis(trimethylsilyl)furan (126386-46-7) + dimethyl acetylenedicarboxylate (762-42-5) → dimethyl 3,4-furandicarboxylate (4282-33-1) + Bis(trimethylsilyl)ethyne (14630-40-1)

Guidance literature:

at 75 ℃;

DOI:10.1039/c39890001238

Reference yield: 23.0%

iodosylbenzene (536-80-1) + 3,4-Bis(trimethylsilyl)furan (126386-46-7) → 4-trimethylsilyl-3-furylphenyliodonium triflate

Guidance literature:

With boron trifluoride diethyl etherate; sodium 2,2,2-trifluoroacetate; In dichloromethane; at 0 ℃; for 3h;

DOI:10.1002/jccs.199900063

upstream raw materials:

4-phenyl-1,3-oxazole

Bis(trimethylsilyl)ethyne

Downstream raw materials:

4-phenyl-3-(trimethylsilyl)furan

4--3-(trimethylsilyl)furan

4-(p-tolyl)-3-(trimethylsilyl)furan

4--3-(trimethylsilyl)furan