trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II)

Base Information

• Chemical Name: trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II)
• CAS No.: 76850-69-6
• Molecular Formula: C₃₂H₄₆N₄O₂PtS₂
• Molecular Weight: 777.955

Synonyms:

Chemical Property of trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II)

There total 4 articles about trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

potassium tetrachloroplatinate(II) (10025-99-7) + N-benzoyl-N’,N’-(di-n-butyl)thiourea (68141-55-9) → cis-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) (76850-69-6,138284-69-2) + trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) (138284-69-2,76850-69-6)

Guidance literature:

With NaCl or NaBr; In ethanol; water; dropwise addn. of hot (70°C) aq. K2PtCl4-soln. (1.01 mmol) to soln. of C6H5CONHCSN(C4H9)2 (2 mmol) in aq. HCl/ethanol in presence of NaCl or NaBr (25 mmol) at 70°C over 10-15 min; stirring for 1 h; cooling in ice;; pptn. of product mixt.; identification by 195-Pt-NMR;;

DOI:10.1016/S0020-1693(00)82866-2

Reference yield:

potassium tetrachloroplatinate(II) (10025-99-7) + N-benzoyl-N’,N’-(di-n-butyl)thiourea (68141-55-9) → cis-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) (76850-69-6,138284-69-2) + trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) (138284-69-2,76850-69-6)

Guidance literature:

With NaCl or NaBr; In ethanol; water; dropwise addn. of hot (70°C) aq. K2PtCl4-soln. (1.01 mmol) to soln. of C6H5CONHCSN(C4H9)2 (2 mmol) in aq. HCl/ethanol in presence of NaCl or NaBr (25 mmol) at 70°C over 10-15 min; stirring for 1 h; cooling in ice;; pptn. of product mixt.; identification by 195-Pt-NMR;;

DOI:10.1016/S0020-1693(00)82866-2

Reference yield:

cis-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) (76850-69-6,138284-69-2) → trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II) (138284-69-2,76850-69-6)

Guidance literature:

In neat (no solvent); the complex retains its isomeric integrity on storage above its melting point (170 ° C) for 30 min;

DOI:10.1039/DT9940000785

upstream raw materials:

hydrogenchloride

potassium tetrachloroplatinate(II)

N-benzoyl-N’,N’-(di-n-butyl)thiourea

cis-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II)

Downstream raw materials:

trans-bis(N,N-di(n-butyl)-N'-benzoylthioureato)platinum(II)

cis-{Pt(C₆H₅CONCSN(C₄H₉)2)(C₆H₅CONHCSN(C₄H₉)2)}I

cis-{Pt(C₆H₅CONCSN(C₄H₉)2)(C₆H₅CONHCSN(C₄H₉)2)}Br

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