Technology Process of cis-3-bromo-3'-methoxy-2',4-dimethyl-5-nitrostilbene
There total 16 articles about cis-3-bromo-3'-methoxy-2',4-dimethyl-5-nitrostilbene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / nitromethane / 22 h / 70 °C
2: 95 percent / sodium borohydride / ethanol / 2 h / Ambient temperature
3: 1.) n-butyllithium / 1.) diethyl ether, hexane, -10 deg C, 1 h; 2.) room temp., 21 h
With
sodium tetrahydroborate; n-butyllithium;
In
nitromethane; ethanol;
DOI:10.1021/jo01294a035
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / tetrahydrofuran / 168 h / Ambient temperature
2: 98 percent / nitromethane / 22 h / 70 °C
3: 95 percent / sodium borohydride / ethanol / 2 h / Ambient temperature
4: n-butyllithium / diethyl ether; hexane / 1.) -10 deg C, 1 h; 2.) r.t., 21 h
With
sodium tetrahydroborate; n-butyllithium;
In
tetrahydrofuran; diethyl ether; nitromethane; ethanol; hexane;
DOI:10.1021/jo01294a035
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / tetrahydrofuran / 168 h / Ambient temperature
2: 98 percent / nitromethane / 22 h / 70 °C
3: 95 percent / sodium borohydride / ethanol / 2 h / Ambient temperature
4: 1.) n-butyllithium / 1.) diethyl ether, hexane, -10 deg C, 1 h; 2.) room temp., 21 h
With
sodium tetrahydroborate; n-butyllithium;
In
tetrahydrofuran; nitromethane; ethanol;
DOI:10.1021/jo01294a035
