N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine

Base Information

Chemical Name:N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine
CAS No.:221656-72-0
Molecular Formula:C₁₈H₂₇N
Molecular Weight:257.419
Hs Code.:

Synonyms:

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Chemical Property of N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine

Chemical Property:

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Technology Process of N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine

There total 7 articles about N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 124-40-3
dimethyl amine

: 221656-71-9
3,7-dimethyl-8-phenyl-2(E),6(E)-octadienyl bromide

: 221656-72-0
N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine

Guidance literature:: In diethyl ether; 0 deg C to rt;
DOI:10.1021/jo981617q

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 221656-72-0
N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 40 percent / SeO₂, tert-butyl hydroperoxide / CH₂Cl₂ / Ambient temperature

2: 96 percent / MnO₂

3: 96 percent / tetrahydrofuran / 1 h / 0 °C

4: ZnBr, NaBH₃CN / 1,2-dichloro-ethane

5: 81 percent / PBr₃

6: 73 percent / diethyl ether / 0 deg C to rt

With tert.-butylhydroperoxide; manganese(IV) oxide; selenium(IV) oxide; phosphorus tribromide; sodium cyanoborohydride; zinc dibromide; In tetrahydrofuran; diethyl ether; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo981617q

Reference yield:

: 37905-03-6
8-hydroxygeranyl acetate

: 221656-72-0
N,N,3,7-tetramethyl-8-phenyl-2(E),6(E)-octadienylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / MnO₂

2: 96 percent / tetrahydrofuran / 1 h / 0 °C

3: ZnBr, NaBH₃CN / 1,2-dichloro-ethane

4: 81 percent / PBr₃

5: 73 percent / diethyl ether / 0 deg C to rt

With manganese(IV) oxide; phosphorus tribromide; sodium cyanoborohydride; zinc dibromide; In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1021/jo981617q