3,5-dimethyl-4b-aza-7H-benzindenoazulene

• Chemical Name: 3,5-dimethyl-4b-aza-7H-benzindenoazulene
• Molecular Formula: C₂₁H₁₇N
• Molecular Weight: 283.373
• Mol file: 98128-24-6.mol

Synonyms:

Chemical Property of 3,5-dimethyl-4b-aza-7H-benz

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-dimethyl-4b-aza-7H-benz

There total 1 articles about 3,5-dimethyl-4b-aza-7H-benzindenoazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

methanol (67-56-1) + ap-9-(2-azido-4,6-dimethylphenyl)fluorene (85681-33-0) → 9-methoxy-9-(2-amino-4,6-dimethylphenyl)fluorene (91481-73-1) + 3,5-dimethyl-4b-aza-7H-benzindenoazulene (98128-24-6) + 4,6-dimethyl-7-(9-fluorenyl)-2-methoxy-3H-azepine (98128-23-5)

Guidance literature:

With sodium methylate; In diethyl ether; at 27 ℃; Product distribution; Irradiation; effect of starting rotamer, variuos temperature, effect of concentration of added base;

DOI:10.1021/ja00308a027

upstream raw materials:

methanol

ap-9-(2-azido-4,6-dimethylphenyl)fluorene