C₂₇H₃₂BF₂N₃O₄

Base Information

• Chemical Name: C₂₇H₃₂BF₂N₃O₄
• CAS No.: 1425860-97-4
• Molecular Formula: C₂₇H₃₂BF₂N₃O₄
• Molecular Weight: 511.377
• Mol file: 1425860-97-4.mol

Synonyms:

Chemical Property of C₂₇H₃₂BF₂N₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of C₂₇H₃₂BF₂N₃O₄

There total 1 articles about C₂₇H₃₂BF₂N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

2,4-dimethyl-1H-pyrrole (625-82-1) + boron trifluoride diethyl etherate (109-63-7) + ehyl 2-[N-ethoxyformyl methyl-N-(4-formylphenyl)]amino acetate (27919-79-5) → C27H32BF2N3O4 (1425860-97-4)

Guidance literature:

2,4-dimethyl-1H-pyrrole; ethyl 2-[N-ethoxyformyl methyl-N-(4-formylphenyl)]aminoacetate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 10h; Inert atmosphere;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 4h; Inert atmosphere;

boron trifluoride diethyl etherate; With triethylamine; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c2dt32531d

Reference yield: 48.0%

C27H32BF2N3O4 (1425860-97-4) + 2,2'-iminobis[ethanol] (111-42-2) → C31H42BF2N5O6 (1425860-99-6)

Guidance literature:

In acetonitrile; for 24h; Inert atmosphere; Reflux;

DOI:10.1039/c2dt32531d

upstream raw materials:

2,4-dimethyl-1H-pyrrole

boron trifluoride diethyl etherate

ehyl 2-[N-ethoxyformyl methyl-N-(4-formylphenyl)]amino acetate

Downstream raw materials:

C₃₁H₄₂BF₂N₅O₆