dichloro bis(benzylamine) palladium (II)

Base Information

Chemical Name:dichloro bis(benzylamine) palladium (II)
CAS No.:55176-74-4
Molecular Formula:C₁₄H₁₈Cl₂N₂Pd
Molecular Weight:391.636
Hs Code.:

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Chemical Property of dichloro bis(benzylamine) palladium (II)

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Technology Process of dichloro bis(benzylamine) palladium (II)

There total 4 articles about dichloro bis(benzylamine) palladium (II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 7440-05-3
palladium

: 100-47-0
benzonitrile

: 19046-92-5,55176-74-4
trans-Cl₂Pd(H₂NCH₂C₆H₅)2

Guidance literature:: With HCl; In ethanol; Electrochem. Process; electrolysis of Pd-foil, HCl, EtOH and benzonitrile at 25 V for 60 min;; evapn. of solvent over a steam bath, cooling to room temp., elem. anal.;
DOI:10.1016/S0277-5387(00)83662-1

Reference yield:

: 187852-72-8,93916-90-6
[Pd(OAc)₂(PhCH₂NH₂)₂]

: 7647-14-5
sodium chloride

: 19046-92-5,55176-74-4
trans-Cl₂Pd(H₂NCH₂C₆H₅)2

Guidance literature:: In water; acetone; for 12h;
DOI:10.1016/j.ica.2017.02.027

Reference yield:

: 14349-67-8
tetrachloropalladium anion

: 100-46-9
benzylamine

: 19046-92-5,55176-74-4
dichloro bis(benzylamine) palladium (II)

Guidance literature:: In water; on react. of benzyl amine with neutral aq. soln. of (PdCl4)(2-), first forming of a weakly reddish ppt. (Vauquelin's salt), which is dissolved in excess benzyl amine (colorless); pptn. on addn. of HCl; washing with cold H2O;;