triphenylantimony difluoride

Base Information

Chemical Name:triphenylantimony difluoride
CAS No.:34716-90-0
Molecular Formula:C₁₈H₁₅F₂Sb
Molecular Weight:391.064
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylantimony difluoride

Chemical Property:

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Technology Process of triphenylantimony difluoride

There total 13 articles about triphenylantimony difluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 603-36-1
triphenylantimony

: 429-06-1
N,N,N,N-tetraethylammonium tetrafluoroborate

: 373-84-2,34716-90-0
difluorotriphenyl-λ⁵-stibane

Guidance literature:: In acetonitrile; Electrolysis; argon atmosphere; cell with diaphragm, anode Pt beaker, cathode Pt wire,reference electrode Ag/AgNO3, anolyte Ph3Sb/Et4NBF4 soln., catholyte satd. PyHBF4 soln., current density 1.67 mA/cm**2, 1.50 Ah electricity passed, 20°C; solvent removal (vac.), residue extn. (ether), crystn. on ether removal, crystals washing (water), recrystn. (ethanol), vac.-drying (60°C); elem. anal.;

Reference yield: 90.0%

: 603-36-1
triphenylantimony

: 73602-61-6,23588-89-8,29585-72-6,94527-74-9
triethylamine tris(hydrogen fluoride)

: 373-84-2,34716-90-0
difluorotriphenyl-λ⁵-stibane

Guidance literature:: In acetonitrile; Electrolysis; N2 atmosphere, ambient temp.; constant current electrolysis (Pt plate and wire electrodes); extraction (ether), washing of extracts (water, brine), drying (MgSO4),solvent removal, recrystn. (ethanol);
DOI:10.1016/S0013-4686(97)85470-9

Reference yield: 84.0%

: 603-36-1
triphenylantimony

: 373-84-2,34716-90-0
difluorotriphenyl-λ⁵-stibane

Guidance literature:: With nitrosonium tetrafluoroborate; In dichloromethane; at 0 - 20 ℃; for 3h; Reagent/catalyst; Solvent;
DOI:10.1016/j.jfluchem.2017.04.004