palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl

Base Information

Chemical Name:palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl
CAS No.:1197358-65-8
Molecular Formula:C₂₂H₁₅ClN₂Pd
Molecular Weight:449.247
Hs Code.:

Synonyms:

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Chemical Property of palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl

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Technology Process of palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl

There total 1 articles about palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: sodium tetrachloropalladate(II)

: 85575-95-7
6,6’-diphenyl-2,2’-bipyridine

: 1197358-65-8
palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl

Guidance literature:: With HCl; In water; to Pd-compd. in H2O added under vigorous stirring pyridine-compd. and 2 N HCl, heated to reflux for 5 days, cooled; filtered, washed with H2O, EtOH and Et2O, recrystallised from CH2Cl2/Et2O, elem. anal.;
DOI:10.1016/j.jorganchem.2009.07.034

Reference yield: 88.0%

: 14104-20-2
silver tetrafluoroborate

: 1197358-65-8
palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl

: 603-35-0
triphenylphosphine

: 1197358-81-8
(palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)(P(C₆H₅)3))(BF₄)

Guidance literature:: In acetone; byproducts: AgCl; AgBF4 added under vigorous stirring to Pd-compd. in acetone, AgCl filtered, solid P(C6H5)3 (molar ratio 1:1) added to the filtered solution, stirred at room temp. for 1 h; concentrated, treated with Et2O, filtered, washed with Et2O, elem. anal.;
DOI:10.1016/j.jorganchem.2009.07.034

Reference yield: 60.0%

: 14104-20-2
silver tetrafluoroborate

: 201230-82-2
carbon monoxide

: 1197358-65-8
palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)Cl

: 1197358-77-2
(palladium(II)(6,6'-diphenyl-2,2'-bipyridine-H)(CO))(BF₄)

Guidance literature:: In acetone; byproducts: AgCl; AgBF4 added under vigorous stirring to Pd-compd. in acetone, AgCl filtered, CO bubbled into the solution at room temp. for 2 h; concentrated to dryness;
DOI:10.1016/j.jorganchem.2009.07.034