2-[(E)-3,3-dimethoxybut-1-enyl]-1,3,3-trimethyl-cyclohexene

Base Information

• Chemical Name: 2-[(E)-3,3-dimethoxybut-1-enyl]-1,3,3-trimethyl-cyclohexene
• CAS No.: 102840-48-2
• Molecular Formula: C₁₅H₂₆O₂
• Molecular Weight: 238.37
• Mol file: 102840-48-2.mol

Synonyms:

Chemical Property of 2-[(E)-3,3-dimethoxybut-1-enyl]-1,3,3-trimethyl-cyclohexene

Chemical Property:

• Vapor Pressure: 0.00219mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[(E)-3,3-dimethoxybut-1-enyl]-1,3,3-trimethyl-cyclohexene

There total 1 articles about 2-[(E)-3,3-dimethoxybut-1-enyl]-1,3,3-trimethyl-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-β-ionone (79-77-6,14901-07-6) + trimethyl orthoformate (149-73-5) → β-Jonon-dimethylketal (102840-48-2)

Guidance literature:

With hydrogenchloride; ethanol; In methanol;

DOI:10.1007/BF00856063

Reference yield: 76.0%

β-Jonon-dimethylketal (102840-48-2) + Sucrose (57-50-1) → (2R,4aR,6R,7R,8R,8aS)-6-((2S,3S,4S,5R)-3,4-Dihydroxy-2,5-bis-hydroxymethyl-tetrahydro-furan-2-yloxy)-2-methyl-2-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

Guidance literature:

With pyridinium p-toluenesulfonate; In N,N-dimethyl-formamide; for 20h; Ambient temperature;

DOI:10.1080/07328309808005773

Reference yield:

β-Jonon-dimethylketal (102840-48-2) → 2-((E)-3-Methoxy-buta-1,3-dienyl)-1,3,3-trimethyl-cyclohexene

Guidance literature:

With toluene-4-sulfonic acid; In quinoline;

DOI:10.1007/BF00856063

upstream raw materials:

(E)-β-ionone

trimethyl orthoformate