C₂₁H₃₂O₃

Base Information

Chemical Name:C₂₁H₃₂O₃
CAS No.:1130279-63-8
Molecular Formula:C₂₁H₃₂O₃
Molecular Weight:332.483
Hs Code.:

C<sub>21</sub>H<sub>32</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₂₁H₃₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₃₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₁H₃₂O₃

There total 9 articles about C₂₁H₃₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: C₂₀H₃₀O₃

: 74-88-4
methyl iodide

: 1130279-63-8
C₂₁H₃₂O₃

Guidance literature:: C₂₀H₃₀O₃; methyl iodide; With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 2h;

methanol; With sodium ethanolate; In N,N-dimethyl-formamide; for 1h;

Reference yield:

: C₂₀H₃₀O₃

: 74-88-4
methyl iodide

: 1130279-63-8
C₂₁H₃₂O₃

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 2h;
DOI:10.1002/asia.201000147

Reference yield:

: 1130279-54-7
C₁₆H₂₄O₂

: 1130279-63-8
C₂₁H₃₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / Reflux

1.2: 4 h / 25 °C

2.1: sodium tetrahydroborate / ethanol / 0.5 h / 0 °C

2.2: 0.5 h / 0 - 25 °C

3.1: sodium tetrahydroborate / ethanol / 1 h / 0 °C

4.1: dmap; triethylamine / dichloromethane / 0.5 h / 0 - 25 °C

5.1: copper(I) iodide-lithium chloride / tetrahydrofuran; diethyl ether / 0.17 h / 25 °C

5.2: 0.5 h / 25 °C

6.1: Jones reagent / acetone / 0.5 h / 25 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 25 °C

With dmap; sodium tetrahydroborate; Jones reagent; copper(I) iodide-lithium chloride; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1002/asia.201000147