tetramesitylporphinato ruthenium(II)(CO)(methanol)

Base Information

Chemical Name:tetramesitylporphinato ruthenium(II)(CO)(methanol)
CAS No.:130461-48-2
Molecular Formula:C₅₈H₅₆N₄O₂Ru
Molecular Weight:942.178
Hs Code.:

Synonyms:

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Chemical Property of tetramesitylporphinato ruthenium(II)(CO)(methanol)

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Technology Process of tetramesitylporphinato ruthenium(II)(CO)(methanol)

There total 1 articles about tetramesitylporphinato ruthenium(II)(CO)(methanol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 5,10,15,20-tetramesitylporphyrin

: 201230-82-2
carbon monoxide

: 10049-08-8,63767-78-2
ruthenium(III)chloride

: 84-58-2
2,3-dicyano-5,6-dichloro-p-benzoquinone

: 130461-48-2
tetramesitylporphinato ruthenium(II)(CO)(methanol)

Guidance literature:: With sodium hydrogensulfite; In dichloromethane; A suspn. of the base in Me(OCH2CH2)2OH was refluxed under CO, a soln. of RuCl3 added, refluxing for 24 h; concg. cooling, addn. of water, filtn., drying, dissolving in CH2Cl2, addn. of DDQ, refluxing, addn. of NaHSO3, column chromy., addn. of MeOH; filtn.;
DOI:10.1016/S0020-1693(00)80216-9

Reference yield:

: 130461-48-2
tetramesitylporphinato ruthenium(II)(CO)(methanol)

: 92669-44-8
dioxo(tetramesitylporphyrinato)ruthenium(VI)

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; dropwise addn. of acid in CH2Cl2 to complex in CH2Cl2, stirred at room temp. for 10 min; column chromy. (Al2O3), evapd., recrystd. from toluene/MeCN;