methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate

Base Information

Chemical Name:methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate
CAS No.:78023-86-6
Molecular Formula:C₁₂H₁₆O₄
Molecular Weight:224.257
Hs Code.:

Synonyms:

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Chemical Property of methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate

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Technology Process of methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate

There total 1 articles about methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3187-58-4
methyl orsellinate

: 75-26-3
isopropyl bromide

: 78023-86-6
methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 26h; Heating;
DOI:10.1039/P19810000883

Reference yield:

: 78023-86-6
methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate

: 78023-84-4
2-(4,6-dihydroxy-3-methoxycarbonyl-2-methylphenoxy)-5-chloro-4-hydroxy-6-methylbenzoic acid

Guidance literature:: Multi-step reaction with 9 steps

1: K₂CO₃ / acetone / 20 h / Heating

2: 15.0 g / TiCl₄ / CH₂Cl₂ / 4 h / 0 °C

3: 9.3 g / TiCl₄ / CH₂Cl₂ / 4.5 h / 0 °C

4: K₂CO₃ / dimethylformamide

5: 3.7 g / sodium chlorite (aq) / dioxane; various solvent(s)

6: 1.8 g / trifluoroacetic anhydride / 1,2-dichloro-ethane / 24 h / Ambient temperature

7: 740 mg / H₂, HCl (aq) / Pd-C / ethyl acetate

8: 600 mg / potassium hexacyanoferrate(III), K₂CO₃ / H₂O / 0.5 h

9: 115 mg / BCl₃ / CH₂Cl₂ / -10 deg C, 15 min -> room temperature, 30 min

With hydrogenchloride; sodium chlorite; hydrogen; boron trichloride; titanium tetrachloride; potassium carbonate; trifluoroacetic anhydride; potassium hexacyanoferrate(III); palladium on activated charcoal; In 1,4-dioxane; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.1039/P19810000883

Reference yield:

: 78023-86-6
methyl 2-hydroxy-4-isopropyloxy-6-methylbenzoate

: 78023-97-9
methyl 3-(3-chloro-4,6-dihydroxy-2-methylbenzoyl)-4-hydroxy-6-methoxy-2-methylbenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: K₂CO₃ / acetone / 20 h / Heating

2: 15.0 g / TiCl₄ / CH₂Cl₂ / 4 h / 0 °C

3: 9.3 g / TiCl₄ / CH₂Cl₂ / 4.5 h / 0 °C

4: K₂CO₃ / dimethylformamide

5: 3.7 g / sodium chlorite (aq) / dioxane; various solvent(s)

6: 1.8 g / trifluoroacetic anhydride / 1,2-dichloro-ethane / 24 h / Ambient temperature

7: 740 mg / H₂, HCl (aq) / Pd-C / ethyl acetate

With hydrogenchloride; sodium chlorite; hydrogen; titanium tetrachloride; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.1039/P19810000883