2,4-dihydroxycyclohexanone dimethylacetal

Base Information

Chemical Name:2,4-dihydroxycyclohexanone dimethylacetal
CAS No.:126325-69-7
Molecular Formula:C₈H₁₆O₄
Molecular Weight:176.213
Hs Code.:

Synonyms:

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Chemical Property of 2,4-dihydroxycyclohexanone dimethylacetal

Chemical Property:

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Technology Process of 2,4-dihydroxycyclohexanone dimethylacetal

There total 1 articles about 2,4-dihydroxycyclohexanone dimethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67-56-1
methanol

: 69125-55-9
4-hydroxy-1-methoxy-1-cyclohexene

: 126325-69-7,126331-48-4
2,4-dihydroxycyclohexanone dimethylacetal

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; for 0.5h; Ambient temperature;

Reference yield:

: 126325-69-7,126331-48-4
2,4-dihydroxycyclohexanone dimethylacetal

: 59096-18-3
(S)-(-)-3'-methoxy-4'-O-methyljoubertiamine

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) CSA, 2.) K₂CO₃ / 1.) RT; 6 h, 0.5 mmHg, 2.) CH₂Cl₂, 10 min

2: 93 percent / PCC, celite / CH₂Cl₂ / 12 h / Ambient temperature

3: 90 percent / tetrahydrofuran

4: 1.) PDC, Ac₂O, molecular sieves 3A, 2.) AcOH / 1.) CH₂Cl₂, RT; 2 h, 2.) 0 deg C, 10 min

5: LiAlH₄, MgBr₂ / diethyl ether / 4 h / -78 °C

6: 90 percent / 1 h / 110 °C

7: 1.) LiAlH₄, 2.) 80percent AcOH, conc. H₂SO₄ / 1.) ether, 0 deg C, 2 h, 2.) H₂O, reflux, 1 h

With lithium aluminium tetrahydride; dipyridinium dichromate; 3 A molecular sieve; Celite; sulfuric acid; camphor-10-sulfonic acid; acetic anhydride; potassium carbonate; acetic acid; pyridinium chlorochromate; magnesium bromide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 126325-69-7,126331-48-4
2,4-dihydroxycyclohexanone dimethylacetal

: 115276-23-8,115305-09-4
2-hydroxy-4-phenyl-3-cyclohexen-1-one (2S,3S)-1,4-dimethoxy-2,3-butylene acetal

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) CSA, 2.) K₂CO₃ / 1.) RT; 6 h, 0.5 mmHg, 2.) CH₂Cl₂, 10 min

2: 93 percent / PCC, celite / CH₂Cl₂ / 12 h / Ambient temperature

3: 90 percent / tetrahydrofuran / 1.) -78 deg C, 2 h, 2.) 0 deg C, 1 h,

4: 1.) PDC, Ac₂O, 2.) Al₂O₃ / 1.) CH₂Cl₂, RT; 2 h, 2.) ether, AcOEt

5: NaBH₄, CeCl₃ / methanol / 4 h / -78 °C

With aluminum oxide; sodium tetrahydroborate; dipyridinium dichromate; cerium(III) chloride; Celite; camphor-10-sulfonic acid; acetic anhydride; potassium carbonate; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane;