2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester

Base Information

Chemical Name:2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester
CAS No.:199382-24-6
Molecular Formula:C₃₁H₄₈O₅S
Molecular Weight:532.785
Hs Code.:

Synonyms:

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Chemical Property of 2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester

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Technology Process of 2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester

There total 11 articles about 2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 629-11-8
1,6-hexanediol

: 199382-24-6
2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 54 percent / NaH / tetrahydrofuran / 2 h / Heating

2: pyridine / CH₂Cl₂ / 72 h / 20 °C

3: 5.10 g / NaI; NaHCO₃ / acetone / 72 h / 20 °C

4: 83 percent / Li₂CuCl₄ / tetrahydrofuran; diethyl ether / 2 h / 0 °C

5: 88 percent / 4-methylmorpholine N-oxide; OsO₄ / H₂O; 2-methyl-propan-2-ol; acetone / 2 h / 20 °C

6: 84 percent / pyridine / CH₂Cl₂ / -78 - 0 °C

7: 46 percent

8: 94 percent / K₂CO₃ / methanol / 2 h / 0 °C

9: pyridine / 72 h / 20 °C

With pyridine; osmium(VIII) oxide; dilithium tetrachlorocuprate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1016/S0040-4020(00)00904-2

Reference yield:

: 71126-73-3
6-benzyloxyhexan-1-ol

: 199382-24-6
2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine / CH₂Cl₂ / 72 h / 20 °C

2: 5.10 g / NaI; NaHCO₃ / acetone / 72 h / 20 °C

3: 83 percent / Li₂CuCl₄ / tetrahydrofuran; diethyl ether / 2 h / 0 °C

4: 88 percent / 4-methylmorpholine N-oxide; OsO₄ / H₂O; 2-methyl-propan-2-ol; acetone / 2 h / 20 °C

5: 84 percent / pyridine / CH₂Cl₂ / -78 - 0 °C

6: 46 percent

7: 94 percent / K₂CO₃ / methanol / 2 h / 0 °C

8: pyridine / 72 h / 20 °C

With pyridine; osmium(VIII) oxide; dilithium tetrachlorocuprate; sodium hydrogencarbonate; potassium carbonate; 4-methylmorpholine N-oxide; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1016/S0040-4020(00)00904-2

Reference yield:

: 97510-97-9
(((6-iodohexyl)oxy)methyl)benzene

: 199382-24-6
2,4,6-Triisopropyl-benzenesulfonic acid (R)-9-benzyloxy-2-hydroxy-nonyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / Li₂CuCl₄ / tetrahydrofuran; diethyl ether / 2 h / 0 °C

2: 88 percent / 4-methylmorpholine N-oxide; OsO₄ / H₂O; 2-methyl-propan-2-ol; acetone / 2 h / 20 °C

3: 84 percent / pyridine / CH₂Cl₂ / -78 - 0 °C

4: 46 percent

5: 94 percent / K₂CO₃ / methanol / 2 h / 0 °C

6: pyridine / 72 h / 20 °C

With pyridine; osmium(VIII) oxide; dilithium tetrachlorocuprate; potassium carbonate; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1016/S0040-4020(00)00904-2