[(W(CO)5)2(PhPHPHPh)]

Base Information

Chemical Name:[(W(CO)5)2(PhPHPHPh)]
CAS No.:1350883-58-7
Molecular Formula:C₂₂H₁₂O₁₀P₂W₂
Molecular Weight:865.979
Hs Code.:

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Chemical Property of [(W(CO)5)2(PhPHPHPh)]

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Technology Process of [(W(CO)5)2(PhPHPHPh)]

There total 5 articles about [(W(CO)5)2(PhPHPHPh)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: (OC)5WP(C₆H₅)C₆H₂(CH₃)2(CO₂CH₃)2

: 2049-55-0
triphenylphosphine borane

: 1350883-58-7,1350883-63-4
[(W(CO)5)2(PhPHPHPh)]

Guidance literature:: With copper(l) chloride; In tetrahydrofuran; at 60 ℃; for 8.5h; Inert atmosphere;
DOI:10.1021/om400637j

Reference yield: 31.3%

: 82265-64-3
syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

: 1333-74-0
hydrogen

: 82839-08-5
(phenylphosphinous acid)pentacarbonyltungsten

: 1350883-58-7,1350883-63-4
[(W(CO)5)2(PhPHPHPh)]

Guidance literature:: In toluene; High Pressure; exposure of tungsten compd. in toluene tp 20 bar of H2, heating at 120°C for 3 h; cooling to room temp., evapn., chromy. (silica gel, 90/10 hexane/CH2Cl2)at 0°C, NMR;
DOI:10.1021/om2009974