N-methyl-N-(2,4-dibromophenyl)sulfuric diamide

Base Information

• Chemical Name: N-methyl-N-(2,4-dibromophenyl)sulfuric diamide
• CAS No.: 127903-07-5
• Molecular Formula: C₇H₈Br₂N₂O₂S
• Molecular Weight: 344.027
• Mol file: 127903-07-5.mol

Synonyms:

Chemical Property of N-methyl-N-(2,4-dibromophenyl)sulfuric diamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methyl-N-(2,4-dibromophenyl)sulfuric diamide

There total 3 articles about N-methyl-N-(2,4-dibromophenyl)sulfuric diamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

2,4-dibromo-N-methylaniline (73557-58-1) → N-methyl-N-(2,4-dibromophenyl)sulfuric diamide (127903-07-5)

Guidance literature:

With sulphamoyl chloride; In benzene; for 1h; Ambient temperature;

Reference yield:

N-methylaniline (100-61-8) → N-methyl-N-(2,4-dibromophenyl)sulfuric diamide (127903-07-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / Br₂ / acetic acid / 0.5 h / 30 °C

2: 58 percent / NH₂SO₂Cl / benzene / 1 h / Ambient temperature

With sulphamoyl chloride; bromine; In acetic acid; benzene;

Reference yield:

methanol (67-56-1) + C7H7Br2N2O2S(1-) → methanolate (3315-60-4) + N-methyl-N-(2,4-dibromophenyl)sulfuric diamide (127903-07-5)

Guidance literature:

at 25 ℃; Equilibrium constant;

upstream raw materials:

methanol

2,4-dibromo-N-methylaniline

N-methylaniline

Downstream raw materials:

sulfamic acid methyl ester

2,4-dibromo-N-methylaniline

methanol

Refernces