1,3-Dimethoxy-1-phenylpropan-2-one

Base Information

Chemical Name:1,3-Dimethoxy-1-phenylpropan-2-one
CAS No.:130895-69-1
Molecular Formula:C11H14O3
Molecular Weight:194.23
Hs Code.:
DSSTox Substance ID:DTXSID10564325
Nikkaji Number:J1.145.736C

Synonyms:1,3-Dimethoxy-1-phenylpropan-2-one;130895-69-1;SCHEMBL8533332;DTXSID10564325

Suppliers and Price of 1,3-Dimethoxy-1-phenylpropan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,3-Dimethoxy-1-phenylpropan-2-one

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:194.094294304
Heavy Atom Count:14
Complexity:173

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COCC(=O)C(C1=CC=CC=C1)OC

Technology Process of 1,3-Dimethoxy-1-phenylpropan-2-one

There total 3 articles about 1,3-Dimethoxy-1-phenylpropan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 67-56-1
methanol

: 99071-90-6
2-methoxy-2-phenylacetyldiazomethane

: 130895-69-1
1-phenyl-1,3-dimethoxy-2-propanone

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4039(99)00995-8

Reference yield:

: 7021-09-2
rac-methoxyphenylacetic acid

: 130895-69-1
1-phenyl-1,3-dimethoxy-2-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 4 h / 60 °C

2: diethyl ether / 1) -2 deg C to 0 deg C, 90 min, 2) room temperature, 1 h

3: BF₃*Et₂O / 1 h / Ambient temperature

With thionyl chloride; boron trifluoride diethyl etherate; In diethyl ether;

Reference yield:

: 34713-98-9,55137-68-3,56271-12-6,39098-93-6
2-methoxy-2-(phenyl)acetyl chloride

: 130895-69-1
1-phenyl-1,3-dimethoxy-2-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 1) -2 deg C to 0 deg C, 90 min, 2) room temperature, 1 h

2: BF₃*Et₂O / 1 h / Ambient temperature

With boron trifluoride diethyl etherate; In diethyl ether;