1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one

Base Information

Chemical Name:1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one
CAS No.:13101-93-4
Molecular Formula:C₁₃H₁₁ClO₂
Molecular Weight:234.682
Hs Code.:
DSSTox Substance ID:DTXSID50579170
Nikkaji Number:J3.198.877B
Wikidata:Q82469606
Mol file:13101-93-4.mol

Synonyms:13101-93-4;1-(5-CHLORO-6-METHOXYNAPHTHALEN-2-YL)ETHANONE;1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one;2-acetyl-5-chloro-6-methoxynaphthalene;SCHEMBL11078616;DTXSID50579170;HZZKQNQXGHJQRF-UHFFFAOYSA-N;5-chloro-6-methoxy-2-acetylnaphthalene;NS00133292;(5-chloro-6-methoxy-2-naphthalenyl)-ethanone;1-(5-Chloro-6-methoxy-naphthalen-2-yl)-ethanone

Suppliers and Price of 1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:234.0447573
Heavy Atom Count:16
Complexity:267

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC2=C(C=C1)C(=C(C=C2)OC)Cl

Technology Process of 1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one

There total 7 articles about 1-(5-Chloro-6-methoxynaphthalen-2-yl)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 13101-92-3
1-chloro-2-methoxynaphthalene

: 75-36-5
acetyl chloride

: 13101-93-4
1-(5-chloro-6-methoxynaphthalen-2-yl)ethan-1-one

Guidance literature:: With cetyltrimethylammonim bromide; cetyltrimethylammonium chloride; In 1,2-dichloro-ethane; at 70 ℃; for 0.0833333h; Microwave irradiation; Micellar solution;
DOI:10.1016/j.tetlet.2013.04.075

Reference yield: 96.0%

: 13101-92-3
1-chloro-2-methoxynaphthalene

: 108-24-7
acetic anhydride

: 13101-93-4
1-(5-chloro-6-methoxynaphthalen-2-yl)ethan-1-one

Guidance literature:: With trifluoroacetic acid; at 100 ℃; for 56h; Inert atmosphere;
DOI:10.1016/j.tetlet.2018.01.026

Reference yield: 87.0%

: 3900-45-6
6-methoxy-2-acetylnaphthalene

: 13101-93-4
1-(5-chloro-6-methoxynaphthalen-2-yl)ethan-1-one

: 1-(5,7-dichloro-6-methoxynaphthalen-2-yl)ethanone

Guidance literature:: With tetraethylammonium chloride; trichloroacetonitrile; In acetonitrile; at 23 ℃; for 2h; Electrochemical reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.1c00704