benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate

Base Information

Chemical Name:benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate
CAS No.:1447194-69-5
Molecular Formula:C₃₃H₂₉NO₅
Molecular Weight:519.597
Hs Code.:

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Chemical Property of benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate

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Technology Process of benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate

There total 3 articles about benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 1447194-69-5
benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; 4-methyl-morpholine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / dichloromethane

2: lithium aluminium tetrahydride / tetrahydrofuran / -25 °C

3: tin(ll) chloride / dichloromethane

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; tin(ll) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201302106

Reference yield:

: 299207-24-2
(9H-fluoren-9-yl)methyl (S)-(1-(methoxy(methyl)amino)-1-oxo-3-phenylpropan-2-yl)carbamate

: 1447194-69-5
benzyl (4S)-4-(N-fmoc)amino-3-oxo-5-phenylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / -25 °C

2: tin(ll) chloride / dichloromethane

With lithium aluminium tetrahydride; tin(ll) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201302106