4-methyl-thiobenzoic acid O-benzyl ester

Base Information

Chemical Name:4-methyl-thiobenzoic acid O-benzyl ester
CAS No.:83078-39-1
Molecular Formula:C₁₅H₁₄OS
Molecular Weight:242.342
Hs Code.:

4-methyl-thiobenzoic acid <i>O</i>-benzyl ester

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Chemical Property of 4-methyl-thiobenzoic acid O-benzyl ester

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Technology Process of 4-methyl-thiobenzoic acid O-benzyl ester

There total 4 articles about 4-methyl-thiobenzoic acid O-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: tert-butyl (4-methylphenylcarbonothioyl)(phenyl)carbamate

: 100-51-6,185532-71-2
benzyl alcohol

: 83078-39-1
4-methyl-thiobenzoic acid O-benzyl ester

Guidance literature:: With potassium phosphate; palladium diacetate; tris(pentafluorophenyl)phosphine; In toluene; at 110 ℃; for 12h; Inert atmosphere; Sealed tube;
DOI:10.1039/d1ob02349g

Reference yield: 70.0%

: 60410-77-7
bis(4-methylbenzenethiocarbonyl) sulphide

: 20194-18-7
sodium phenyl-methanolate

: 5467-99-2
4-methylbenzoic acid benzyl ester

: 83078-39-1
4-methyl-thiobenzoic acid O-benzyl ester

: 53724-36-0
sodium 4-(methyl)dithiobenzoate

Guidance literature:: In diethyl ether; ethanol; at 0 ℃; for 3h;

Reference yield:

: 4294-57-9
para-methylphenylmagnesium bromide

: 83078-39-1
4-methyl-thiobenzoic acid O-benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 2 h / 0 - 20 °C / Sealed tube; Inert atmosphere

2: dmap / acetonitrile / 15 h / 20 °C / Sealed tube; Inert atmosphere

3: palladium diacetate; tris(pentafluorophenyl)phosphine; potassium phosphate / toluene / 12 h / 110 °C / Inert atmosphere; Sealed tube

With dmap; potassium phosphate; palladium diacetate; tris(pentafluorophenyl)phosphine; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1039/d1ob02349g