N-Benzoxybenzolsulfonamid

Base Information

Chemical Name:N-Benzoxybenzolsulfonamid
CAS No.:22172-70-9
Molecular Formula:C₁₂H₁₁NO₃S
Molecular Weight:249.29
Hs Code.:

Synonyms:

Suppliers and Price of N-Benzoxybenzolsulfonamid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzoxybenzolsulfonamid

Chemical Property:

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Safty Information:

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Technology Process of N-Benzoxybenzolsulfonamid

There total 3 articles about N-Benzoxybenzolsulfonamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4846-21-3
O-phenylhydroxylamine

: 98-09-9
benzenesulfonyl chloride

: 22172-70-9
N-Benzoxybenzolsulfonamid

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/acs.oprd.9b00002

Reference yield:

: 64908-64-1
2-phenoxyisoindol-1,3-dione

: 22172-70-9
N-Benzoxybenzolsulfonamid

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / methanol; chloroform / 12 h / 20 °C

2: triethylamine / dichloromethane / 12 h / 20 °C

With hydrazine hydrate; triethylamine; In methanol; dichloromethane; chloroform;
DOI:10.1021/acs.oprd.9b00002

Reference yield:

: 98-80-6
phenylboronic acid

: 22172-70-9
N-Benzoxybenzolsulfonamid

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 20 °C / Molecular sieve

2: hydrazine hydrate / methanol; chloroform / 12 h / 20 °C

3: triethylamine / dichloromethane / 12 h / 20 °C

With pyridine; hydrazine hydrate; triethylamine; copper(l) chloride; In methanol; dichloromethane; chloroform; 1,2-dichloro-ethane;
DOI:10.1021/acs.oprd.9b00002