(((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂

Base Information

Chemical Name:(((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂
CAS No.:635684-06-9
Molecular Formula:C₆₂H₅₆Cl₂O₄P₂Pt
Molecular Weight:1193.06
Hs Code.:

(((CH<sub>2</sub>CHC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>OC<sub>6</sub>H<sub>4</sub>)2PCH<sub>2</sub>)2)PtCl<sub>2</sub>

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Chemical Property of (((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂

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Technology Process of (((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂

There total 1 articles about (((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 12080-32-9
dichloro( 1,5-cyclooctadiene)platinum(ll)

: 92434-51-0
1-bromo-4-((4-vinylbenzyl)oxy)benzene

: 28240-69-9
1,2-bis(dichlorophosphino)ethane

: 635684-06-9
(((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂

Guidance literature:: With n-butyllithium; copper(l) chloride; In tetrahydrofuran; hexane; dichloromethane; to arylbromide in THF at -78°C soln. n-BuLi in hexane was added, -78°C for 1 h, CuCl was added, 15 min, soln. Cl2PCH2CH2PCl2 in THF was added, -78°C for 24 h under Ar, (COD)PtCl2 in CH2Cl2 was added, 1 h at room temp.; volatiles were removed in vacuo, residue was taken up in CH2Cl2, filtered, and evapd., residue was washed with Et2O;
DOI:10.1021/om0340387

Reference yield: 72.0%

: 635684-06-9
(((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)PtCl₂

: silver carbonate

: 635684-07-0
(((CH₂CHC₆H₄CH₂OC₆H₄)2PCH₂)2)Pt(CO₃)

: silver(I) chloride

Guidance literature:: In dichloromethane; to soln. Pt complex in CH2Cl2 Ag2CO3 was added and stirred at room temp.protected from light for 8 h; soln. was filtered, slvent was evapd.;
DOI:10.1021/om0340387