C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si

Base Information

Chemical Name:C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si
CAS No.:1396507-32-6
Molecular Formula:C₂₄H₃₉FN₂O₂Si
Molecular Weight:433.671
Hs Code.:

C<sub>24</sub>H<sub>39</sub><sup>(18)</sup>FN<sub>2</sub>O<sub>2</sub>Si

Synonyms:

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Chemical Property of C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si

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Technology Process of C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si

There total 7 articles about C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1396506-65-2
di-tert-butyl(3-((tert-butyldimethylsilyloxy)methyl)-4-methoxyphenyl)fluorosilane

: 1396507-32-6
C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / methanol; water / 19 h / 20 °C

2: pyridinium chlorochromate / dichloromethane / 20 °C / Cooling with ice

3: potassium permanganate / dichloromethane; tert-butyl alcohol / 3 h / 20 °C / pH 3 / aq. phosphate buffer

4: pyridine; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / chloroform / 22 h / 0 - 20 °C

5: [¹⁸F]-hydrofluoric acid; tetrabutylammonium bicarbonate / acetonitrile / 0.08 h / 20 °C

With [¹⁸F]-hydrofluoric acid; pyridine; hydrogenchloride; potassium permanganate; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; pyridinium chlorochromate; tetrabutylammonium bicarbonate; In methanol; dichloromethane; chloroform; water; acetonitrile; tert-butyl alcohol;
DOI:10.3390/molecules16097458

Reference yield:

: 1396506-79-8
5-(di-tert-butylfluorosilyl)-2-methoxybenzaldehyde

: 1396507-32-6
C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: potassium permanganate / dichloromethane; tert-butyl alcohol / 3 h / 20 °C / pH 3 / aq. phosphate buffer

2: pyridine; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / chloroform / 22 h / 0 - 20 °C

3: [¹⁸F]-hydrofluoric acid; tetrabutylammonium bicarbonate / acetonitrile / 0.08 h / 20 °C

With [¹⁸F]-hydrofluoric acid; pyridine; potassium permanganate; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; tetrabutylammonium bicarbonate; In dichloromethane; chloroform; acetonitrile; tert-butyl alcohol;
DOI:10.3390/molecules16097458

Reference yield:

: 80866-82-6
5-bromo-2-methoxy-benzyl alcohol

: 1396507-32-6
C₂₄H₃₉⁽¹⁸⁾FN₂O₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1H-imidazole / dichloromethane / 20 h / 20 °C

2.1: tert.-butyl lithium / diethyl ether / 0.17 h / -78 °C

2.2: 19 h / -78 - 20 °C

3.1: hydrogenchloride / methanol; water / 19 h / 20 °C

4.1: pyridinium chlorochromate / dichloromethane / 20 °C / Cooling with ice

5.1: potassium permanganate / dichloromethane; tert-butyl alcohol / 3 h / 20 °C / pH 3 / aq. phosphate buffer

6.1: pyridine; 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / chloroform / 22 h / 0 - 20 °C

7.1: [¹⁸F]-hydrofluoric acid; tetrabutylammonium bicarbonate / acetonitrile / 0.08 h / 20 °C

With [¹⁸F]-hydrofluoric acid; pyridine; 1H-imidazole; hydrogenchloride; potassium permanganate; 1-hydroxy-pyrrolidine-2,5-dione; tert.-butyl lithium; dicyclohexyl-carbodiimide; pyridinium chlorochromate; tetrabutylammonium bicarbonate; In methanol; diethyl ether; dichloromethane; chloroform; water; acetonitrile; tert-butyl alcohol;
DOI:10.3390/molecules16097458