RuCl₃(4'-(C₆H₄-p-N(C₁₆H₃₃)2)-2,2':6',2''-terpyridine)

Base Information

• Chemical Name: RuCl₃(4'-(C₆H₄-p-N(C₁₆H₃₃)2)-2,2':6',2''-terpyridine)
• CAS No.: 1377788-38-9
• Molecular Formula: C₅₃H₈₀Cl₃N₄Ru
• Molecular Weight: 980.674

Synonyms:

Chemical Property of RuCl₃(4'-(C₆H₄-p-N(C₁₆H₃₃)2)-2,2':6',2''-terpyridine)

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of RuCl₃(4'-(C₆H₄-p-N(C₁₆H₃₃)2)-2,2':6',2''-terpyridine)

There total 1 articles about RuCl₃(4'-(C₆H₄-p-N(C₁₆H₃₃)2)-2,2':6',2''-terpyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

4'-[4-(N,N-dihexadecylamino)phenyl]-2,2':6',2''-terpyridine + ruthenium trichloride hydrate (14898-67-0) → RuCl3(4'-(C6H4-p-N(C16H33)2)-2,2':6',2''-terpyridine) (1377788-38-9)

Guidance literature:

In not given; soln. ligand in MeOH or abs. EtOH was added to soln. RuCl3*xH2O in the same solvent, refluxed for 4 h and left at room temp. overnight; ppt. was filtered off, washed with cold MeOH or abs. EtOH and dried in vacuo; elem. anal.;

DOI:10.1039/c2dt30183k

Reference yield: 78.0%

4'-[4-(N,N-dihexadecylamino)phenyl]-2,2':6',2''-terpyridine + RuCl3(4'-(C6H4-p-N(C16H33)2)-2,2':6',2''-terpyridine) (1377788-38-9) + silver 4-ethylbenzoate (870814-23-6) → [Ru(4'-(C6H4-p-N(C16H33)2)-2,2':6',2''-terpyridine)2][4-EtC6H4COO]2

Guidance literature:

With N-ethylmorpholine; In ethanol; byproducts: AgCl; soln. ligand in abs EtOH and 5 drops N-ethylmorpholine was added to soln. Ru complex in abs. EtOH, refluxed for 1 h, soln. was filtered hot through Celite, soln. 4-EtC6H4COOAg in hot EtOH was added, stirred at room temp. overnight; soln. was filtered through Celite and evapd.; elem. anal.;

DOI:10.1039/c2dt30183k

Reference yield: 70.0%

RuCl3(4'-(C6H4-p-N(C16H33)2)-2,2':6',2''-terpyridine) (1377788-38-9) + silver 4-ethylbenzoate (870814-23-6) + 4’-(4-nitrophenyl)-2,2’,6’,2’’-terpyridine (129077-51-6) → [Ru(4'-(C6H4-p-N(C16H33)2)-2,2':6',2''-terpyridine)(4'-(C6H4-p-NO2)-2,2':6',2''-terpyridine)][4-EtC6H4COO]2

Guidance literature:

With N-ethylmorpholine; In ethanol; byproducts: AgCl; soln. ligand in abs EtOH and 5 drops N-ethylmorpholine was added to soln. Ru complex in abs. EtOH, refluxed for 1 h, soln. was filtered through Celite, soln. 4-EtC6H4COOAg in hot EtOH was added, stirred at room temp.overnight; soln. was filtered through Celite and evapd.; elem. anal.;

DOI:10.1039/c2dt30183k

upstream raw materials:

ruthenium trichloride hydrate

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