3-butyl-1-methyl-1,2-diphenyl-1-stannaindene

Base Information

Chemical Name:3-butyl-1-methyl-1,2-diphenyl-1-stannaindene
CAS No.:896728-04-4
Molecular Formula:C₂₅H₂₆Sn
Molecular Weight:445.191
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-butyl-1-methyl-1,2-diphenyl-1-stannaindene

Chemical Property:

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Technology Process of 3-butyl-1-methyl-1,2-diphenyl-1-stannaindene

There total 3 articles about 3-butyl-1-methyl-1,2-diphenyl-1-stannaindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 896728-02-2
3-butyl-1,1,2-triphenyl-1-stannaindene

: 74-88-4
methyl iodide

: 896728-04-4
3-butyl-1-methyl-1,2-diphenyl-1-stannaindene

: 104110-08-9
3-butyl-1,1-dimethyl-2-phenyl-1-stannaindene

Guidance literature:: With Li; In diethyl ether; byproducts: C6H5Li; (Ar); ether was added to mixt. of Sn compd. and Li (2.5 equiv.) at room temp.; stirred for 4 h; MeI was added; filtered; volatiles removed; chromd. (gel permeation); elem. anal.;
DOI:10.1021/om050879x

Reference yield:

: 1135-99-5
diphenyltin(IV) dichloride

: 896728-04-4
3-butyl-1-methyl-1,2-diphenyl-1-stannaindene

Guidance literature:: Multi-step reaction with 2 steps

1: (CH₃)2NC₂H₄N(CH₃)2 / hexane; tetrahydrofuran

2: Li / diethyl ether

With (CH₃)2NC₂H₄N(CH₃)2; Li; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/om050879x

Reference yield:

: 501-65-5
diphenyl acetylene

: 896728-04-4
3-butyl-1-methyl-1,2-diphenyl-1-stannaindene

: 104110-08-9
3-butyl-1,1-dimethyl-2-phenyl-1-stannaindene

Guidance literature:: Multi-step reaction with 2 steps

1: (CH₃)2NC₂H₄N(CH₃)2 / hexane; tetrahydrofuran

2: Li / diethyl ether

With (CH₃)2NC₂H₄N(CH₃)2; Li; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/om050879x