Technology Process of C29H26Cl2O
There total 3 articles about C29H26Cl2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: Dess-Martin periodane / dichloromethane / 24 h / 20 °C / Inert atmosphere
2: tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
With
Dess-Martin periodane;
In
tetrahydrofuran; dichloromethane;
2: Grignard reaction;
DOI:10.1002/ejoc.201001484
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; sulfuric acid; copper; ammonium chloride; copper(l) chloride / 3 h
1.2: 168 h / 20 °C / Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 24 h / 20 °C / Inert atmosphere
3.1: tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; sulfuric acid; copper; ammonium chloride; Dess-Martin periodane; copper(l) chloride;
In
tetrahydrofuran; dichloromethane;
3.1: Grignard reaction;
DOI:10.1002/ejoc.201001484
- Guidance literature:
-
In
tetrahydrofuran;
at 0 - 20 ℃;
for 6h;
optical yield given as %de;
Inert atmosphere;
DOI:10.1002/ejoc.201001484