C₁₅H₂₁ClO₂Si

Base Information

Chemical Name:C₁₅H₂₁ClO₂Si
CAS No.:1643478-52-7
Molecular Formula:C₁₅H₂₁ClO₂Si
Molecular Weight:296.869
Hs Code.:

C<sub>15</sub>H<sub>21</sub>ClO<sub>2</sub>Si

Synonyms:

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Chemical Property of C₁₅H₂₁ClO₂Si

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Technology Process of C₁₅H₂₁ClO₂Si

There total 5 articles about C₁₅H₂₁ClO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1643478-50-5
(E)-3-(3-(tert-Butyldimethylsilyloxy)-2-chlorophenyl)prop-2-en-1-ol

: 1643478-52-7
C₁₅H₂₁ClO₂Si

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c4ob00250d

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1643478-52-7
C₁₅H₂₁ClO₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.25 h / -78 - 0 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene; 2.1: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1039/c4ob00250d

Reference yield:

: 56962-10-8
2-chloro-3-hydroxybenzaldehyde

: 1643478-52-7
C₁₅H₂₁ClO₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.75 h / 0 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.25 h / -78 - 0 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene; 2.1: |Horner-Wadsworth-Emmons Olefination / 2.2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1039/c4ob00250d