Technology Process of C23H29N3O5S
There total 4 articles about C23H29N3O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1021/jm200733r
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; ammonium formate / ethanol / 3 h / 23 °C / Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 23 °C / Inert atmosphere
3: sodium hydroxide / diethyl ether; dichloromethane; water; ethyl acetate / 18 h / Inert atmosphere
4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
With
lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; ammonium formate; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; ethyl acetate;
4: Mitsunobu reaction;
DOI:10.1021/jm200733r
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide / diethyl ether; dichloromethane; water; ethyl acetate / 18 h / Inert atmosphere
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
With
di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate;
2: Mitsunobu reaction;
DOI:10.1021/jm200733r
