[(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

Base Information

Chemical Name:[(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]
CAS No.:1345735-66-1
Molecular Formula:C₂₇H₂₃FeMnO₅
Molecular Weight:538.262
Hs Code.:

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Chemical Property of [(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

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Technology Process of [(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

There total 2 articles about [(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 12093-10-6
ferrocenecarboxaldehyde

: 1190934-69-0,1312165-63-1,1312165-66-4
[(η5-MeOC6H4BrPh)Mn(CO)3]

: 1345735-66-1
[(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

: [(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

Guidance literature:: With CH₃CH₂CH₂CH₂Li; In tetrahydrofuran; treatment with butyllithium in THF at -78°C, treatment with ferrocene deriv. in THF at -78°C;
DOI:10.1021/om200905p

Reference yield: 50.0%

: 12093-10-6
ferrocenecarboxaldehyde

: 81857-39-8
(η5-2-methoxy-6-phenylcyclohexadienyl)Mn(CO)3

: 1345735-66-1
[(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

Guidance literature:: With C₄H₉Li; (CH₃)2NCH₂CH₂N(CH₃)2; In tetrahydrofuran; treatment of manganese compd. with butyllithium and TMEDA in THF at -78°C, treatment with ferrocene deriv. in THF at -78°C;
DOI:10.1021/om200905p

Reference yield: 54.0%

: 1345735-66-1
[(η5-MeOC6H4(Ph)CH(OH)Fc)Mn(CO)3]

: 67969-83-9
tetrafluoroboric acid dimethyl ether complex

: 1345735-76-3
[(η5-MeOC6H4(Ph)CHFc)Mn(CO)3]BF4

Guidance literature:: In dichloromethane; treatment of manganese compd. with 3 equiv. of HBF4*dimethyl ether in CH2Cl2 at room temp.;
DOI:10.1021/om200905p