2-methyl-dodecanoic acid methyl ester

Base Information

Chemical Name:2-methyl-dodecanoic acid methyl ester
CAS No.:149948-65-2
Molecular Formula:C₁₄H₂₈O₂
Molecular Weight:228.375
Hs Code.:

Synonyms:

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Chemical Property of 2-methyl-dodecanoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-methyl-dodecanoic acid methyl ester

There total 2 articles about 2-methyl-dodecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 112-41-4,25067-08-7,62132-67-6
1-dodecene

: 201230-82-2
carbon monoxide

: 1731-88-0
methyl tridecanoate

: 55554-08-0,149948-65-2,149948-76-5
2-methyl-dodecanoic acid methyl ester

Guidance literature:: With copper dichloride; palladium on activated charcoal; at 25 ℃; for 192h; under 760 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1246/bcsj.64.3600

Reference yield:

: 67-56-1
methanol

: 112-41-4,25067-08-7,62132-67-6
1-dodecene

: 1731-88-0
methyl tridecanoate

: 74810-60-9
2-ethyl-undecanoic acid methyl ester

: 55554-08-0,149948-65-2,149948-76-5
2-methyl-dodecanoic acid methyl ester

: Methyl-α-propyl-decanoat

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; tetrabutylammomium bromide; water; toluene-4-sulfonic acid; at 110 ℃; for 2h; under 22502.3 Torr;
DOI:10.1134/S096554411006006X

Reference yield:

: 55554-08-0,149948-65-2,149948-76-5
2-methyl-dodecanoic acid methyl ester

: Toluene-4-sulfonic acid 2-methyl-dodecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LiAlH₄; 2.) HCl / 1.) diethyl ether, 8 h, reflux; 2.) 0 deg C, water

2: pyridine / 1 h / 0 °C

With hydrogenchloride; lithium aluminium tetrahydride; In pyridine;