[(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄)

Base Information

Chemical Name:[(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄)
CAS No.:926321-40-6
Molecular Formula:C₄₈H₃₇CuN₇*ClO₄
Molecular Weight:874.865
Hs Code.:

[(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO<sub>4</sub>)

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Chemical Property of [(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄)

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Technology Process of [(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄)

There total 1 articles about [(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14057-91-1
tetrakis(acetonitrile)copper(I) perchlorate

: 926321-29-1
tris(3,5-diphenyl-1-pyrazolyl)methane

: 926321-40-6
[(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄)

Guidance literature:: In tetrahydrofuran; under Ar; to a soln. of a ligand in THF was added Cu-contg. compd. (1 equiv.); the mixt. was stirred for several hours and ambient temp.; the soln. was filtered; pentane was added to the filtrate with stirring to ppt. the complex; recrystn. from CH3CN/Et2O;
DOI:10.1021/ic060745r

Reference yield: 79.0%

: 75-09-2
dichloromethane

: 926321-40-6
[(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(acetonitrile)](ClO₄)

: 201230-82-2
carbon monoxide

: [(tris(3,5-diphenyl-1-pyrazolyl)methane)Cu(CO)](ClO₄)*0.5(dichloromethane)

Guidance literature:: In dichloromethane; under Ar; a Cu-contg. compd. was dissolved in a min. amt. of CH2Cl2; thesoln. was stirred under atm. of CO for 1 h at ambient temp.; diffusion of Et2O into the soln. for crystn. of the solid; elem. anal.;
DOI:10.1021/ic060745r