ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate

Base Information

Chemical Name:ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate
CAS No.:179110-31-7
Molecular Formula:C₂₀H₁₇ClO₆
Molecular Weight:388.804
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate

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Technology Process of ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate

There total 3 articles about ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23468-31-7
6-chloropiperonyl chloride

: 6296-54-4
ethyl 2,4-dioxo-4-phenylbutyrate

: 179110-31-7
ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate

Guidance literature:: With sodium ethanolate; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1016/S0960-894X(00)00513-8

Reference yield:

: 98-86-2
acetophenone

: 179110-31-7
ethyl beta-benzoyl 6-chloro alpha-oxo-1,3-benzodioxol 5-butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOEt / ethanol / 20 h / 0 - 20 °C

2: NaOEt; NaI / dimethylformamide / 16 h / 20 °C

With sodium ethanolate; sodium iodide; In ethanol; N,N-dimethyl-formamide; 1: Condensation / 2: Alkylation;
DOI:10.1016/S0960-894X(00)00513-8