2-iodo 3,4,5,6-tetrafluoro phenyllithium

Base Information

Chemical Name:2-iodo 3,4,5,6-tetrafluoro phenyllithium
CAS No.:1036240-41-1
Molecular Formula:C₆F₄ILi
Molecular Weight:281.905
Hs Code.:

Synonyms:

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Chemical Property of 2-iodo 3,4,5,6-tetrafluoro phenyllithium

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Technology Process of 2-iodo 3,4,5,6-tetrafluoro phenyllithium

There total 1 articles about 2-iodo 3,4,5,6-tetrafluoro phenyllithium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5488-71-1
tetrafluorobezyne

: 10377-51-2
lithium iodide

: 1036240-41-1
2-iodo 3,4,5,6-tetrafluoro phenyllithium

Guidance literature:

Reference yield: 93.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1036240-41-1
2-iodo 3,4,5,6-tetrafluoro phenyllithium

: 1643-19-2
tetrabutylammomium bromide

: 1036240-32-0
NBu₄[Au(2-iodotetrafluorophenyl)2]

Guidance literature:: In diethyl ether; Au complex added to soln. of Li compd. at 203 K in Et2O; mixt. stirred for 1 h; Bu4NBr added; mixt. stirred at 203 K for 40 min and at room temp. for 20 h; solid filtered off and washed with H2O, Et2O and n-hexane; dissolved in CH2Cl2; soln. concd. under vac.; pptd. by addn. of n-hexane; elem. anal.;
DOI:10.1021/om8000586

Reference yield:

: 1036240-41-1
2-iodo 3,4,5,6-tetrafluoro phenyllithium

: (NBu₄[Tl(Au(2-iodotetrafluorophenyl)2)2])n

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: tetrahydrofuran

In tetrahydrofuran; diethyl ether;
DOI:10.1021/om8000586