2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate

Base Information

Chemical Name:2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate
CAS No.:1335128-06-7
Molecular Formula:C₂₃H₂₄O₅S
Molecular Weight:412.507
Hs Code.:

Synonyms:

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Chemical Property of 2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate

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Technology Process of 2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate

There total 4 articles about 2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1335128-06-7
2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine / toluene / Reflux

2: cetyltrimethylammonim bromide; sodium hydroxide / dichloromethane / 80 °C

3: sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; sodium hydroxide / 20 °C

4: triethylamine / dichloromethane / 2 h / 20 °C

With piperidine; sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; cetyltrimethylammonim bromide; triethylamine; sodium hydroxide; In dichloromethane; toluene; 1: Knoevenagel condensation;
DOI:10.1111/j.1747-0285.2011.01093.x

Reference yield:

: 7786-61-0,31853-85-7
3-methoxy-4-hydroxystyrene

: 1335128-06-7
2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: cetyltrimethylammonim bromide; sodium hydroxide / dichloromethane / 80 °C

2: sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; sodium hydroxide / 20 °C

3: triethylamine / dichloromethane / 2 h / 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; cetyltrimethylammonim bromide; triethylamine; sodium hydroxide; In dichloromethane;
DOI:10.1111/j.1747-0285.2011.01093.x

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1335128-06-7
2-(3-methoxy-4-benzyloxyphenyl)ethyl tosylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / dimethyl sulfoxide / 20 °C

2: sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; sodium hydroxide / 20 °C

3: triethylamine / dichloromethane / 2 h / 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; dihydrogen peroxide; sodium hydride; triethylamine; sodium hydroxide; In dichloromethane; dimethyl sulfoxide; 1: Wittig reaction;
DOI:10.1111/j.1747-0285.2011.01093.x