C₅₁H₅₃NO₉

Base Information

Chemical Name:C₅₁H₅₃NO₉
CAS No.:1391912-05-2
Molecular Formula:C₅₁H₅₃NO₉
Molecular Weight:823.983
Hs Code.:

C<sub>51</sub>H<sub>53</sub>NO<sub>9</sub>

Synonyms:

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Chemical Property of C₅₁H₅₃NO₉

Chemical Property:

Purity/Quality:

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Technology Process of C₅₁H₅₃NO₉

There total 7 articles about C₅₁H₅₃NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1391912-05-2
C₅₁H₅₃NO₉

Guidance literature:: Multi-step reaction with 6 steps

1: 18-crown-6 ether; potassium carbonate / acetone / 24 h / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C

3: phosphorus tribromide / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

4: 18-crown-6 ether; potassium carbonate / N,N-dimethyl-formamide; acetone / 24 h / Inert atmosphere; Reflux

5: water; sodium hydroxide / tetrahydrofuran; methanol / 18 h / 65 °C

6: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 24 h / 25 °C / Inert atmosphere

With lithium aluminium tetrahydride; 18-crown-6 ether; tetrabutyl ammonium fluoride; water; phosphorus tribromide; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ma300654j

Reference yield:

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1391912-05-2
C₅₁H₅₃NO₉

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; [N,N'-bis(salicylidene)-1,2-ethanediaminato]Mn(III) chloride / isopropyl alcohol / 24 h

2: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 24 h / 25 °C / Inert atmosphere

With sodium tetrahydroborate; [N,N'-bis(salicylidene)-1,2-ethanediaminato]Mn(III) chloride; tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/ma300654j

Reference yield:

: 176038-84-9
3,5-dipropargyloxybenzyl alcohol

: 1391912-05-2
C₅₁H₅₃NO₉

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus tribromide / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

2: 18-crown-6 ether; potassium carbonate / N,N-dimethyl-formamide; acetone / 24 h / Inert atmosphere; Reflux

3: water; sodium hydroxide / tetrahydrofuran; methanol / 18 h / 65 °C

4: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 24 h / 25 °C / Inert atmosphere

With 18-crown-6 ether; tetrabutyl ammonium fluoride; water; phosphorus tribromide; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ma300654j