Chalkon-epoxid

Base Information

Chemical Name:Chalkon-epoxid
CAS No.:7570-85-6
Molecular Formula:C₁₅H₁₂O₂
Molecular Weight:224.259
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Chalkon-epoxid

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Technology Process of Chalkon-epoxid

There total 116 articles about Chalkon-epoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 614-47-1
1,3-diphenyl-propen-3-one

: 5411-12-1,7570-85-6,7570-86-7,61840-92-4,61840-93-5,67381-79-7,70332-63-7
trans-(2S,3R)-epoxy-1,3-diphenylpropan-1-one

Guidance literature:: With Cumene hydroperoxide; 4 A molecular sieve; Triphenylphosphine oxide; chiral bis[(S)-BINOL] La(III); In tetrahydrofuran; at 25 ℃; for 0.5h;
DOI:10.1002/anie.200501676

Reference yield: 99.0%

: 94-41-7
benzalacetophenone

: 5411-12-1,7570-85-6,7570-86-7,61840-92-4,61840-93-5,67381-79-7,70332-63-7
trans-(2S,3R)-epoxy-1,3-diphenylpropan-1-one

Guidance literature:: With sodium hypochlorite; (6R,6"R,2R,2"R)-6,6"-dimethyldispiro[tetrahydropyran-2,2'-(2,3,4,6,7,8-hexahydro-1H-pyrimido[1,2-a]pyrimidine)-8',2"-tetrahydropyran]-9'-ium tetrafluoroborate; In water; toluene; at 0 - 20 ℃; for 16h; Reagent/catalyst; enantioselective reaction; Catalytic behavior;
DOI:10.1016/j.tet.2015.11.058

Reference yield: 98.0%

: 100-52-7
benzaldehyde

: 98-86-2
acetophenone

: 5411-12-1,7570-85-6,7570-86-7,61840-92-4,61840-93-5,67381-79-7,70332-63-7
trans-(2S,3R)-epoxy-1,3-diphenylpropan-1-one

Guidance literature:: benzaldehyde; acetophenone; at 60 ℃; for 3h;

With tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide; In toluene; at 20 ℃; for 1.5h; enantioselective reaction;
DOI:10.1016/j.jcat.2015.11.020