monomethylammonium p-toluenesulfonate

Base Information

• Chemical Name: monomethylammonium p-toluenesulfonate
• CAS No.: 2840-20-2
• Molecular Formula: CH₅N*C₇H₈O₃S
• Molecular Weight: 203.262
• Mol file: 2840-20-2.mol

Synonyms:

Chemical Property of monomethylammonium p-toluenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of monomethylammonium p-toluenesulfonate

There total 6 articles about monomethylammonium p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

acetamide (60-35-5) + [hydroxy(tosyloxy)iodo]benzene (27126-76-7) → monomethylammonium p-toluenesulfonate (2840-20-2)

Guidance literature:

In acetonitrile; for 15h; Mechanism; Product distribution; Heating; other carboxamides; var. time;

DOI:10.1021/jo00364a010

Reference yield:

toluene (108-88-3,15644-74-3,16713-13-6) → monomethylammonium p-toluenesulfonate (2840-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid

2: water

With sulfuric acid; water;

Reference yield:

C53H60INO12*C7H8O3S*CH5N → monomethylammonium p-toluenesulfonate (2840-20-2) + C53H60INO12 (182305-75-5)

Guidance literature:

In chloroform-d1; at 26.9 ℃; Equilibrium constant; stability constants of other calix<4>arene complexes with other neutral molecules and ammonium ions, other solvent: CCl4;

DOI:10.1021/jo960937b

upstream raw materials:

acetamide

[hydroxy(tosyloxy)iodo]benzene

toluene

Downstream raw materials:

cotinine

3-methylamino-1-thiophen-2-yl-propan-1-one p-toluenesulfonate

Refernces

• 1、 Arduini, Arturo,McGregor, William M.,Pochini, Andrea,Secchi, Andrea,Ugozzoli, Franco,Ungaro, Rocco. "New upper rim pyridine-bridged calix[4]arenes: Synthesis and complexation properties toward neutral molecules and ammonium ions in organic media". . p. 6881 - 6887. Retrieved 2007/10/03.