2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate

Base Information

Chemical Name:2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate
CAS No.:147529-17-7
Molecular Formula:C₁₉H₂₂O₃S
Molecular Weight:330.448
Hs Code.:

Synonyms:

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Chemical Property of 2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate

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Technology Process of 2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate

There total 3 articles about 2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85591-54-4
2-tert-butylsulfanyl-1-phenylethanone

: 147529-17-7
2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol / 48 h / Ambient temperature

2: 1.) pyridine / 1.) CH₂Cl₂, -4 deg C, 5-10 min, 2.) 0 deg C, 1.5 h

With pyridine; sodium tetrahydroborate; In ethanol;
DOI:10.1021/jo00058a007

Reference yield:

: 70-11-1
α-bromoacetophenone

: 147529-17-7
2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium hydride / 1.) THF, 0 deg C, 10 min, 2. THF, a) 0 deg C, 40 min, b) r.t., 1.5 h

2: NaBH₄ / ethanol / 48 h / Ambient temperature

3: 1.) pyridine / 1.) CH₂Cl₂, -4 deg C, 5-10 min, 2.) 0 deg C, 1.5 h

With pyridine; sodium tetrahydroborate; sodium hydride; In ethanol;
DOI:10.1021/jo00058a007

Reference yield:

: 120886-76-2
2-((2-methyl-2-propyl)thio)-1-phenylethanol

: 1885-14-9
phenyl chloroformate

: 147529-17-7
2-((2-methyl-2-propyl)thio)-1-phenylethyl phenyl carbonate

Guidance literature:: With pyridine; Yield given. Multistep reaction; 1.) CH₂Cl₂, -4 deg C, 5-10 min, 2.) 0 deg C, 1.5 h;
DOI:10.1021/jo00058a007